Chemical Properties:
Package: Fluorinated Bottle, Aluminium foil bag, 25kg/Cardboard Drum, or according to customer's requirement. Storage Condition: Hygroscopic. Store in sealed containers at cool, dry and ventilated warehouse away from incompatible substances. Protect from light and moisture. Store away from strong oxidizing agents. Shanghai Ruifu Chemical Co., Ltd. is the leading manufacturer and supplier of Glycinamide Hydrochloride (H-Gly-NH2·HCl) (CAS: 1668-10-6) with high quality, production capacity 200 Tons per year, it is sold to domestic and foreign markets, well received by our customers. We can provide worldwide delivery, small and bulk quantities available. If you are interested in Glycinamide Hydrochloride, Please contact: alvin@ruifuchem.com| Hazard Codes | Xi | F | 3-10 |
| Risk Statements | 36/37/38 | Hazard Class | Irritant |
| Safety Statements | 22-24/25-37/39-26 | HS Code | 2924199090 |
| WGK Germany | 3 |
Description:
Safety Information:
Package & Storage:
| Chemical Name | Glycinamide Hydrochloride |
| Synonyms | H-Gly-NH2·HCl; Gly-NH2·HCl; Glycinamide HCl; 2-Aminoacetamide Hydrochloride |
| Stock Status | In Stock, Production Capacity 200 Tons per Year |
| CAS Number | 1668-10-6 |
| Molecular Formula | C2H6N2O·HCl |
| Molecular Weight | 110.54 |
| Melting Point | 200.0~205.0℃ |
| Density | 1.122 |
| Sensitive | Hygroscopic |
| Water Solubility | Easily Soluble in Water |
| Storage Temp. | Sealed in Dry, Store at Room Temperature |
| COA & MSDS | Available |
| Classification | Amino Acids & Derivatives |
| Brand | Ruifu Chemical |
Advantages:
How to Purchase? Please contact Dr. Alvin Huang: sales@ruifuchem.com or alvin@ruifuchem.com 15 Years Experience? We have more than 15 years of experience in the manufacture and export of a wide range of high quality pharmaceutical intermediates or fine chemicals. Main Markets? Sell to domestic market, North America, Europe, India, Korea, Japanese, Australia, etc. Advantages? Superior quality, affordable price, professional services and technical support, fast delivery. Quality Assurance? Strict quality control system. Professional equipment for analysis include NMR, LC-MS, GC, HPLC, ICP-MS, UV, IR, OR, K.F, ROI, LOD, MP, Clarity, Solubility, Microbial limit test, etc. Samples? Most products provide free samples for quality evaluation, shipping cost should be paid by customers. Factory Audit? Factory audit welcome. Please make an appointment in advance. MOQ? No MOQ. Small order is acceptable. Delivery Time? If within stock, three days delivery guaranteed. Transportation? By Express (FedEx, DHL), by Air, by Sea. Documents? After sales service: COA, MOA, ROS, MSDS, etc. can be provided. Custom Synthesis? Can provide custom synthesis services to best fit your research needs. Payment Terms? Proforma invoice will be sent first after confirmation of order, enclosed our bank information. Payment by T/T (Telex Transfer), PayPal, Western Union, etc.FAQ:
Stable Supply: Maintain reasonable stock
Professional Service: One stop purchasing service
Technical Support: Technology solution available
Custom Synthesis Service: Ranged from grams to kilos
Fast Delivery: If within stock, three days delivery guaranteed
High Quality: Established a complete quality assurance system
Sufficient Capacity: Sufficient facilities and technicians
OEM Package: Custom package and label available
Specifications:
| Items | Inspection Standards | Results |
| Appearance | White Crystal Powder | Conforms |
| Melting Point | 200.0~205.0℃ | 201.4~203.6℃ |
| Heavy Metals (Pb) | ≤10ppm | <10ppm |
| Loss on Drying | ≤0.50% (105℃) | 0.28% |
| Residue on Ignition | ≤0.10% | 0.08% |
| Glycine | ≤1.00% (TLC) | Conforms |
| Assay | 99.0 to 101.0% | 100.06% |
| Infrared Spectrum | Conforms to Structure | Conforms |
| Proton NMR Spectrum | Conforms to Structure | Conforms |
| Conclusion | This Product by Inspection Accords with the Standard In-House | |
| Main Uses | Pharmaceutical Intermediates; Buffer | |
Application:
Glycinamide Hydrochloride (H-Gly-NH2·HCl) (CAS: 1668-10-6) is a buffer that is useful in the physiological pH range. And it is also used as a pharmaceutical intermediate, in the organic synthesis, used for peptide coupling. The product is cyclized with glyoxal to obtain 2-hydroxy pyrazine, and then chlorinated with phosphorus trichloroxy to obtain 2, 3-dichloropyrazine, used in the production of sulfonamides SMPZ. Synthesis route: It is obtained by amination of methyl chloroacetate. The a mmonia water was cooled to below 0℃, and me thyl chloroacetate was added, and the temperature was kept for 2h. A mmonia was passed to a predetermined amount at a temperature below 20℃, and the remaining a mmonia was eliminated after 8h of standing reaction, then the concentration was raised to 60℃ under reduced pressure to obtain Glycinamide Hydrochloride.Package & Storage:
Melting point: Capillary determination method. Should be 200.0~205.0℃ The sample was ground into powder of about 0.1g and dried in a blast oven at 105℃ for half an hour, then loaded into a capillary tube and packed. When the oil temperature in the melting point instrument rises to 190℃, put the capillary into it and control the heating rate at 3℃ per minute. Observe the initial melting point of the contents of the capillary and continue heating until all the contents in the capillary melt to the final melting point. Content: Titration by AgNO3 Weigh the sample 0.2000g, dissolve it in distilled water and dilute it to 100ml, add 3-5 drops of potassium chromate indicator, and titrate with 0.1000M standard silver nitrate to the end point. Calculation: Content %=V×M÷G×0.1105×100 V- Volume consumed by standard silver nitrate titration in ml M- standard silver nitrate concentration mol/L G- Weigh the sample g Moisture measurement: K-F method: Add 10ml anhydrous methanol into the precision moisture meter, titrate K-F reagent with water equivalent greater than 3mg/ml to the end point, quickly sample 1.0000g, put into the above anhydrous methanol, titrate with K-F reagent to the end point; Record the titration volume ml. Calculation: Moisture =V×N÷G×100÷1000 N--The water equivalent of the K-F reagent mg/ml V---The volume consumed by the K-F reagent titration ml G-- Weigh the sample g